Synthesis and X-ray characterization of Li(1–2x)NixTiO(PO4) (0<=x<=0.50)

B. Manoun (1) , Abdelaziz El Jazouli (1) , Pierre Gravereau (2) , Jean-Pierre Chaminade (2)

1 Laboratoire de Chimie des Matériaux Solides
2 ICMCB - Institut de Chimie de la Matière Condensée de Bordeaux

Li(1–2x)NixTiO(PO4) oxyphosphate powders were prepared from dilute solutions of NiCl2·6H2O, Li2CO3, (NH4)2HPO4, and TiCl4 in ethanol. The final temperature was 850 °C. Li(1–2x)NixTiO(PO4) oxyphosphates with 0<=x<=0.10 crystallize in the orthorhombic system with space group Pnma, while those with 0.10

Mots clés: Oxyphosphates; X-ray diffraction; Li(1-2x)NixTiO(PO4)

Domaines: Matériaux

B. Manoun, Abdelaziz El Jazouli, Pierre Gravereau, Jean-Pierre Chaminade. Synthesis and X-ray characterization of Li(1–2x)NixTiO(PO4) (0<=x<=0.50). Powder Diffraction, 2003, 18 (4), pp.301-305. ⟨10.1154/1.1596631⟩. ⟨hal-00165790⟩