TOTAL VALORISATION OF RED CEDAR (THUJA PLICATA) SAWMILLS WASTES. ISOLATION OF EXTRACTIVES AND PRODUCTION OF ACTIVATED CARBON FROM THE SOLID RESIDUE

Hamid Mellouk (1) , Lotfi Khezami (2) , Sid-Ahmed Rezzoug (1) , Richard Capart (2)

1 LEPTIAB - Laboratoire d'Étude des Phénomènes de Transfert et de l'Instantanéité : Agro-industrie et Bâtiment
2 TIMR - Transformation Intégrée de la Matière Renouvelable

Experiments were performed to evaluate a recent extraction process called the instantaneous controlled pressure drop process (briefly: DIC process: “Détente Instantanée Contrôlée”) for extracting some volatile compounds from red cedar wood. This process involves subjecting red cedar chips for a short time (30 s to 5 min) under a steam pressure (1 to 6 bars or from 100 to 165 °C). This first step is followed by a flash decompression toward vacuum (up to 50 mbar). This transition induces a fast evaporation of water and volatile compounds and a cooling effect. The effects of two processing parameters (steam pressure and heating time) on the total extraction yield and on yield of four volatile compounds were evaluated by response surface methodology. The results indicated that the processing pressure is the predominant parameter for global extraction yield of oil (E.O= Extracted Oil) and for yield of the four compounds investigated in this study. The processing time is also a significant parameter but less than processing pressure. Moreover, activated carbon produced from DIC-treated residue revealed larger pore sizes compared to untreated samples.

Mots clés: : Instantaneous controlled pressure drop (DIC Process); Isolation; Extractives; Red cedar (Thuja plicata); Volatiles; Wood; Hydrotreatment; Activated carbon

Domaines: Génie des procédés

Hamid Mellouk, Lotfi Khezami, Sid-Ahmed Rezzoug, Richard Capart. TOTAL VALORISATION OF RED CEDAR (THUJA PLICATA) SAWMILLS WASTES. ISOLATION OF EXTRACTIVES AND PRODUCTION OF ACTIVATED CARBON FROM THE SOLID RESIDUE. BioResouces, 2008, 3 (4), pp.1156-1172. ⟨hal-00414425⟩