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Les produits sont révélés grâce à une lampe UV (254 nm ou 366 nm) ou en utilisant des révélateurs spécifiques 1 . Les composés possédant une amine sont révélés à la Ninhydrine. Les acides hydroxamiques sont révélés au FeCl 3 . Les composés contenant un alcyne terminal sont révélés à l'I 2 . Les séparations par chromatographie sur colonne sont réalisées sur gel de silice 70-230 mesh en utilisant 30-40 ,
N1-(5-(2-(9H-carbazol-9-yl)acetamido)pentyl)-N1-hydroxy-N4-(5-(N- hydroxy-4-(5-(N-hydroxyacetamido)pentylamino)-4- oxobutanamido)pentyl)succinamide, p.435 ,
50 g ; 0,41 mmol) dissous dans 5 mL de DMF (diméthylformamide) sont ajoutés la triéthylamine (0,75 mL, mmol). La solution est laissée sous agitation à température ambiante pendant 4 jours, pp.57-3275 ,
01 (s, 9H, CH 3 )62 (m, 12H, CH2O et CH 2 -CH 2 -COO), RMN 1 H (DMSO, 250 MHz, pp.3548-30898252105 ,
les micro-ondes ont su se démocratiser et prouver leurs utilités dans tous les domaines de la chimie organique, inorganique et la chimie des matériaux hybrides. On les retrouve par exemple dans la génération de liaison C-hétéroatome4, la chimie hétérocyclique 7 , la « click chemistry ,
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est une formation destinée à faciliter l'insertion professionnelle des docteurs Son objectif est de les aider à faire le point sur les compétences et savoir-faire professionnels développés au cours de la préparation de leur doctorat et à se les approprier. Ceci constitue souvent un véritable "challenge" pour les doctorants qui éprouvent des difficultés à discerner et à mettre en avant des acquis tels que la conduite de projet, la gestion du temps, le montage de partenariats, etc. Ce travail de réflexion et d'analyse n'a pas de valeur académique, et peut être rédigé dans un style plus personnel que celui de la thèse ,
La chimie organique m'a été présentée comme un jeu de construction, dans lequel les molécules sont comme des briques de Lego ,
Chimie de l'ULCO m'a permis d'effectuer un stage de recherche à Glasgow en ,
Outre le perfectionnement de mon anglais, ce stage m'a permis de découvrir l'univers de la recherche en chimie organique, du travail de bibliographie au travail de laboratoire, avec ses réussites et ses échecs. Ce stage m'a conforté dans ma poursuite d'étude vers une première année de Master à l'Université de Rouen, master réputé pour son bon niveau en chimie organique ,
ai effectué mon stage de recherche au Laboratoire de Synthèse Organique et Environnement (LSOE) sous la direction du Dr Francine Cazier sur l'émergence d'un nouveau thème de recherche pour le laboratoire qui sera par la suite ,