Pitfalls of a structure determination: The structure of closo -9-[4-(dibenzylamino)phenyl]-1,2-dicarbadodecaborane(12) - Archive ouverte HAL Accéder directement au contenu
Article Dans Une Revue Acta crystallographica Section E : Crystallographic communications [2015-...] Année : 2022

Pitfalls of a structure determination: The structure of closo -9-[4-(dibenzylamino)phenyl]-1,2-dicarbadodecaborane(12)

Résumé

Automated X-ray data recording and data reduction strategies are straightforward and powerful these days, as well as semi-automated routines to solve standard structures without, or at least with only little manual intervention and within a relatively short time. The structure determination of the amino-carborane closo -9-[4-(dibenzylamino)phenyl]-1,2-dicarbadodecaborane(12), C 22 H 29 B 10 N, is an example that automated routines still always have to be revised and that it may be necessary to be aware of possible problems of a structure determination.
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hal-03875823 , version 1 (28-11-2022)

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Max Milewski, Anne-Marie Caminade, Evamarie Hey-Hawkins, Peter Lönnecke. Pitfalls of a structure determination: The structure of closo -9-[4-(dibenzylamino)phenyl]-1,2-dicarbadodecaborane(12). Acta crystallographica Section E : Crystallographic communications [2015-..], 2022, 78 (12), pp.1145-1150. ⟨10.1107/S205698902201043X⟩. ⟨hal-03875823⟩
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