Comparative study of directional solidification of Al-7 wt% Si alloys in Space and on Earth: Effects of gravity on dendrite growth and Columnar-to-equiaxed transition

Yuze Li (1) , Nathalie Mangelinck-Noël (1) , G. Zimmermann (2) , L. Sturz (3) , Henri Nguyen-Thi (1)

1 IM2NP - Institut des Matériaux, de Microélectronique et des Nanosciences de Provence
2 ACCESS (GERMANY)
3 ACCESS (GERMANY)

Directional solidification experiments of grain refined Al −7 wt% Si alloy were carried out on Earth under normal gravity conditions (1 g) and in the Material Science Laboratory on board the International Space Station in microgravity environment (μg), to investigate the impact of the gravity on the solidification microstructure and the columnar-to-equiaxed transition (CET). The increase of the dendrite growth velocity imposed by the processing conditions during the experiments leads to a size decrease of the dendrite microstructure and to a more homogeneous eutectic distribution under both 1 g and μg conditions. A progressive CET is obtained in both samples implying the existence of an intermediate region after the inception position of CET defined as the end of growth of the columnar dendrites. However, a more progressive CET and longer dendrites aligned with the applied temperature gradient are observed in presence of gravity. This difference is attributed to the convective flow on Earth. On the one hand, it carries the grains that nucleate ahead of the columnar front away into the bulk liquid phase. On the other hand, it sweeps the solute away from the dendrite tip zone. Consequently, the blocking effect is diminished, allowing extended continuous growth of the elongated dendrites.

Mots clés: A2 Microgravity conditions; A1 Directional solidification; B1 Alloys; A1 convection; collumnar to equiaxed transition

Domaines: Matériaux

Yuze Li, Nathalie Mangelinck-Noël, G. Zimmermann, L. Sturz, Henri Nguyen-Thi. Comparative study of directional solidification of Al-7 wt% Si alloys in Space and on Earth: Effects of gravity on dendrite growth and Columnar-to-equiaxed transition. Journal of Crystal Growth, 2019, 513, pp.20-29. ⟨hal-02050669⟩