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Direct Analysis Laser Machine ,
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Selected experimental conditions: ablated surface 300 µm × 1 mm; sample translation speed 5 µm s-1 ; scanner speed (laser on) 200 mm s-1 ; scanner speed (laser off) 100 mm s-1 ; He flow rate 570 mL min-1. (38) Gonzalez, Spectrochim. Acta, Part B, vol.63, pp.277-286, 2008. ,
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, of the ablation cell on the elemental concentrations of sediment PACS-2 obtained by in-cell fs-LA-ICP-IDMS. Selected experimental conditions: ablated surface 300 µm × 1 mm; sample translation speed 5 µm s-1 ; scanner speed (laser on) 200 mm s-1 ; scanner speed (laser off) 100 mm s-1. Standard deviation values are calculated from the mean of eight analyses using three independent pellets for both the CRM and the solid spike
, a Standard deviation values for in-cell fs-LA-ICP-IDMS analyses are calculated from the mean of thirty-nine measurements in three independent pellets for both the CRMs and the solid spike. b Indicative noncertified value is also given for information
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, Particle size distribution and structure of the laser-generated aerosol after in-cell fs-LA-ICP-IDMS analysis of sediment PACS-2. (a) Particle size distribution of the generated aerosol measured by ELPI. (b) SEM images of the collected aerosol particles using two scanner speeds (100 and 500 mm s-1 , respectively). These images show the different kinds of transported particles observed for each scanner speed