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Synthesis of GeSe4 glass by mechanical alloying and sintering

Abstract : The possibility to synthesize GeSe4 glass by mechanical alloying followed by sintering has been demonstrated. X-ray diffraction (XRD) and differential scanning calorimetry (DSC) analysis have been performed on the powder as a function of milling duration in order to follow the amorphization process of raw metallic germanium and selenium elements. Completely amorphous powder has been sintered using a homemade hot press. Optical transmission and the density of the final bulk material have been studied
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https://hal.archives-ouvertes.fr/hal-01023627
Contributor : Corinne Perier <>
Submitted on : Tuesday, July 15, 2014 - 8:36:30 AM
Last modification on : Friday, July 10, 2020 - 4:24:52 PM

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Elena Petracovschi, Mathieu Hubert, Jean-Luc Adam, Xianghua Zhang, Laurent Calvez. Synthesis of GeSe4 glass by mechanical alloying and sintering. physica status solidi (b), Wiley, 2014, 251 (7), pp.1330-1333. ⟨10.1002/pssb.201350232⟩. ⟨hal-01023627⟩

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