Mechanical characterization and comparison of different NiTi/silicone rubber interfaces

Thierry Rey 1 Florence Razan 2 Eric Robin 3 Sylvain Faure 2 Jean-Benoît Le Cam 3 Grégory Chagnon 1, * Aurélie Girard 4 Denis Favier 1
* Corresponding author
1 TIMC-IMAG-BioMMat - Ingénierie Biomédicale et Mécanique des Matériaux
TIMC-IMAG - Techniques de l'Ingénierie Médicale et de la Complexité - Informatique, Mathématiques et Applications, Grenoble - UMR 5525
2 SATIE-BIOMIS - Bio-MIcroSystèmes et BioSensors
SIAME - Systèmes d'Information et d'Analyse Multi-Echelles
Abstract : This paper investigates the effects of different surface treatments on the mechanical resistance of interface between wires of NiTi shape memory alloy and silicone rubber. Three different treatments were used; primer, plasma and combination of both. The wires deoxidation effects have also been studied. In order to characterize the interface properties in such composite material, pull-out tests were carried out by means of a home-made device. This test allows us to evaluate the mechanical resistance of the interface in terms of the maximum force reached during the test. First, results show that the debonding force is not higher after the wires deoxidation. This preparation is therefore not necessary. Second, using a primer PM820 and plasma separately leads to a significant improvment of the mechanical resistance. Third, the combination of these treatments (primer followed by plasma) and a longer time of exposure to the plasma alone get the debonding force higher. Consequently, NiTi/silicone rubber interface improved only by means of plasma offers a new way to obtain biocompatible interfaces in such composite material.
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Thierry Rey, Florence Razan, Eric Robin, Sylvain Faure, Jean-Benoît Le Cam, et al.. Mechanical characterization and comparison of different NiTi/silicone rubber interfaces. International Journal of Adhesion and Adhesives, Elsevier, 2014, 48, pp.67-74. ⟨10.1016/j.ijadhadh.2013.09.028⟩. ⟨hal-00963798⟩

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