Backbone assignment of fully protonated solid proteins by 1H detection and ultrafast magic-angle-spinning NMR spectroscopy

Alessandro Marchetti (1, 2) , Stefan Jehle (1) , Michèle Felletti (1) , Michael J. Knight (1) , Yao Wang (3) , Zhi-Qiang Xu (3) , Ah Young Park (4) , Gottfried Otting (4) , Anne Lesage (1) , Nicholas E. Dixon (3) , Guido Pintacuda (1)

1 ISA - Centre de RMN à très hauts champs
2 SNS - Scuola Normale Superiore di Pisa
3 School of Chemistry [Wollongong]
4 Research School of Chemistry

Mots clés: DNA polymerase; magic-angle spinning; NMR spectroscopy; protein structures; scalar transfers; STATE NMR; TERMINAL DOMAIN; MAS; RESOLUTION; PEPTIDES; STRUCTURAL BASIS

Domaines: Chimie théorique et/ou physique

Alessandro Marchetti, Stefan Jehle, Michèle Felletti, Michael J. Knight, Yao Wang, et al.. Backbone assignment of fully protonated solid proteins by 1H detection and ultrafast magic-angle-spinning NMR spectroscopy. Angewandte Chemie International Edition, 2012, 51 (43), pp.10756-10759. ⟨10.1002/anie.201203124⟩. ⟨hal-00809214⟩