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50; S, 7.64%; IR (KBr) m (cm À1CO); MS (DCI/NH 3 ): m/z 409 [M+H + ]; 31 P{ 1 H} NMR (CDCl 3 ): d (ppm): À21.6 (s), Hz, SH, vol.3338, issue.7, pp.164022909206-7 ,
10 (broad s, 1H, NH), p.35 ,
ReO{Ph-P(Ph 2 )N 2 S}] (4) was crystallised by slow evaporation of a CH 2 Cl 2 /hexane solution. A purple crystal of 4 thus produced was mounted on a Nonius Kappa CCD diffractometer equipped with a CDD detector, and was used for data collection. X-ray intensity data were collected with References, Chem. Soc. Rev. Top. Curr. Chem, vol.4, issue.176, pp.43-79, 1996. ,
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Re(1)?N(1) 1.981(6) C(6)?P(1) 1.806(6) Re(1)?S(1) 2.2614(17) Bond angles O(3)?Re(1)?N(1) 113, ) N(2)?Re(1)?N(1) 78.9(2) O(3)?Re(1)?P(1) 106) P(1)?Re(1)?S(1), pp.3-4 ,