| HAL: hal-00709665, version 1 |
| DOI: 10.1016/j.matchar.2012.04.020 |
| Detailed view | Export this paper |
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| Materials Characterization 70 (2012) Pages 28-32 |
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| Fast in-situ annealing stage coupled with EBSD: A suitable tool to observe quick recrystallization mechanisms |
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| Nathalie Bozzolo 1Suzanne Jacomet 1 |
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| (2012-08) |
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| A heating stage has been developed to perform in-situ annealing in a SEM equipped with an EBSD system in order to study recrystallization mechanisms. High temperature treatments could then be performed inside the SEM, up to 1180 °C and with high heating and cooling rates (~ 100 °C s− 1). Samples were cooled down to room temperature to perform EBSD orientation mapping in between successive short-duration heat treatments. Microstructure evolution snapshots obtained this way allow gaining an insight into recrystallization mechanisms. The interest of such experiments is shown for two examples: static recrystallization of cold deformed pure tantalum and post‐dynamic evolution of hot-deformed Zircaloy4. |
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| 1: | Centre de Mise en Forme des Matériaux (CEMEF) |
| CNRS : UMR7635 – MINES ParisTech - École nationale supérieure des mines de Paris | |
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| Subject | : | Engineering Sciences/Materials |
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| EBSD – In-situ annealing – Recrystallization – Tantalum – Zirconium |
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| Attached file list to this document: | |||||
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| hal-00709665, version 1 | |
| http://hal-ensmp.archives-ouvertes.fr/hal-00709665 | |
| oai:hal-ensmp.archives-ouvertes.fr:hal-00709665 | |
| From: Brigitte Hanot | |
| Submitted on: Wednesday, 22 August 2012 15:22:47 | |
| Updated on: Wednesday, 22 August 2012 15:31:46 | |