Quantification and localization of the liquid zone of partially remelted M2 tool steel using X-ray microtomography and scanning electron microscopy

G. C. Gu (1, 2) , Raphaël Pesci (1) , Eric Becker (2) , Laurent Langlois (2) , Régis Bigot (2) , Mario Scheel (3)

1 LEM3 - Laboratoire d'Etude des Microstructures et de Mécanique des Matériaux
2 LCFC - Laboratoire de Conception Fabrication Commande
3 ESRF - European Synchrotron Radiation Facility

Thixoforming of steels poses challenges due to the high temperatures involved and the lack of understanding of thermomechanical behavior. The volume fractions of the liquid and solid phases in the semi-solid state are the most important parameters for such a form-ing process, as they affect the viscosity and hence the flow behavior of the material. Two-dimensional observations might not always be sufficient, as the size distribution and the connectivity of phases cannot be obtained from associated measurements, which can only be determined by three-dimensional (3-D) investigation. This paper presents the first application of high-energy X-ray microtomography to the microstructure of steel in the semi-solid state. The microstructure of M2 high-speed tool steel was studied in both as-received and heated-and-quenched states. From the reconstructed images, 3-D information could be obtained and was compared with scanning elec-tron microscopy and energy dispersive spectrometry observations. The volume fraction and the location of liquid phase in the semi-solid state were determined in particular, and the continuous solid skeleton was investigated.

Mots clés: Semi-solid steel forming; Thermomechanical behavior; X-ray microtomography

Domaines: Matériaux; Matériaux et structures en mécanique [physics.class-ph]; Matériaux et structures en mécanique [physics.class-ph]; Mécanique des matériaux [physics.class-ph]; Mécanique des matériaux [physics.class-ph]

G. C. Gu, Raphaël Pesci, Eric Becker, Laurent Langlois, Régis Bigot, et al.. Quantification and localization of the liquid zone of partially remelted M2 tool steel using X-ray microtomography and scanning electron microscopy. Acta Materialia, 2012, 60 (3), pp.948-957. ⟨10.1016/j.actamat.2011.10.039⟩. ⟨hal-00959514⟩