On-line determination of aggregate size and morphology in suspensions

Michel Cournil (1, 2, 3) , Frédéric Gruy (1, 2, 3) , Patrick Cugniet (1, 2, 3)

1 SPIN-ENSMSE - Centre Sciences des Processus Industriels et Naturels
2 GENERIC - Géochimie, environnement, écoulement, réacteurs industriels et cristallisation
3 LPMG-EMSE - Laboratoire des Procédés en Milieux Granulaires

Information about the aggregation state of fine particles is an important element for process control, product quality monitoring and fundamental understanding in many cases of industrial slurries. When aggregates are small or fragile objects, their withdrawal is difficult and off-line characterization may be a source of error. This work deals with the application of different in line methods to the characterization of silica aggregate size and morphology. These methods are based on turbidimetry. One of them consists of the analysis of the turbidity fluctuations and is operated on a commercial instrument. The other one uses the aggregate settling velocity which is determined by turbidimetry too, however with a home-made apparatus. This work gives us the opportunity to define morphological models for small aggregates and to calculate their drag coefficient. Thanks to these models, the aggregate morphological characteristics and the number of their constituting particles can be derived from the experimental results. Agreement between the different methods is examined and discussed.

Mots clés: Aggregation state; process control; characterization of silica aggregate; turbidimetry; home-made apparatus

Domaines: Génie des procédés

Michel Cournil, Frédéric Gruy, Patrick Cugniet. On-line determination of aggregate size and morphology in suspensions. 9e congrès de la SFGP. "Du rayonnement scientifique à la diffusion des technologies", Sep 2003, Saint-Nazaire, France. C2-9 pp. 71-78. ⟨hal-00839630⟩