Growth and characterization of ferrite film prepared by pulsed laser deposition
Résumé
Ba2Fe12O19 (BaO.6Fe2O3) films have been grown on (0001) sapphire substrate using pulsed laser deposition (PLD) technique. Prepared films were characterized by X-ray diffraction (XRD), X-ray photoelectron spectroscopy (XPS), X-ray reflectivity (XRR), atomic force microscopy (AFM) and magnetic measurements. XRD confirms the formation of Ba2Fe12O19 phase, whereas presence of Fe2O3 was also identified. X-ray photoelectron spectroscopy (XPS) shows the signature of all the elements present in the barium ferrite. XRR data show the thickness of the film is ~ 24.2 nm with top layer roughness of ~ 3.7 nm. AFM measurement suggests the formation of clusters with average roughness of ~ 3.9 nm. Magnetic measurements of the target reveal its anisotropic nature with coercivity values: 0.23 and 0.24 T, obtained along two orthogonal directions. For the prepared thin film, the obtained coercivity ~ 80 mT and saturation induction 0.13 T are lower than the usual values obtained for Ba2Fe12O19 compound (coercivity and saturation induction values are 0.19 Tesla and 0.48 T respectively), can be ascribed to the presence of Fe2O3 phase.
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