A new index to estimate the strain rate sensitivity of glassy polymers using conical/pyramidal indentation

Guillaume Kermouche (1) , Jean-Luc Loubet (1) , Jean-Michel Bergheau (1)

1 LTDS - Laboratoire de Tribologie et Dynamique des Systèmes

The increasing use of polymeric materials as thin coatings requires appropriate mechanical characterization methods taking account of time-dependent effects. A well-known result is that a constant indentation strain rate allows to determine the mechanical properties of such solids from indentation tests. To do that, most people assume a power law creep behavior and use the viscoplasticity index to determine the strain rate sensitivity. In the first part of this paper, we investigate the influence of the indentation strain rate on the hardness of power law creep solids and elastic-viscoplastic solids. It is shown that the assumption of power law creep solid is not sufficient to describe the behavior of polymeric materials in indentation. In the second part, we propose a new index, the EVP index, which gives a better approximation of the strain rate sensitivity than the viscoplasticity index. In the last part, we apply this method to nanoindentation tests on PMMA and polycarbonate samples.

Mots clés: Physical Sciences

Guillaume Kermouche, Jean-Luc Loubet, Jean-Michel Bergheau. A new index to estimate the strain rate sensitivity of glassy polymers using conical/pyramidal indentation. Philosophical Magazine, 2006, 86 (33-35), pp.5667-5677. ⟨10.1080/14786430600778682⟩. ⟨hal-00513712⟩